Nitric Acid, ASTM A, Practice C, (Huey Test) The specimens are boiled for five periods, each of 48 hours, in a 65 per cent solution of nitric acid. The corrosion. employed to measure the relative susceptibility of austenitic stainless steels to intergranular attack. ASTM A Practice C, boiling nitric acid test is also known . Ferric Sulfate – Sulfuric Acid, ASTM A – Practice B (Stretcher Test). Ferric Sulfate Nitric Acid, ASTM A, Practice C, (Huey Test). Nitric Acid, ASTM A

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The test is generally performed for acceptance of materials, but not sufficient for rejection of materials. Please share this page: The samples are weighed at each interval to determine mass loss and degree of susceptibility to intergranular attack. To understand intergranular corrosion testing or intergranular attack commonly abbreviated as IGC or IGAit is important to understand what causes the process to occur.

Intergranular Corrosion Testing: An Overview of ASTM A262

These tests are often run as a qualification test to ensure each batch of stainless steel praftice properly prepared. It is typically used for stainless alloys such as andCr-Ni-Mo stainless alloys, and nickel alloys to evaluate the intergranular attack associated with the precipitation of chromium carbides at grain boundaries. Practice A, the oxalic acid etch test is used as a rapid technique to screen samples of certain stainless steel grades to ensure they are not susceptible to intergranular attack sensitization.

See Appendix X1 for information regarding test selection. ASTM does not give any warranty express or implied or make any representation that the contents of this abstract are accurate, complete practics up to date.

The inch-pound equivalents are in parentheses and may be approximate. Practice E, the Strauss test, is performed to assess attack associated with chromium-rich carbide prwctice it does not detect susceptibility to sigma phase formation.


The ASTM A tests can determine if the proper heat treatment was performed or if the alloys are in danger of intergranular corrosion occurring in use. Work Item s – proposed revisions of this standard. Please specify the maximum allowable corrosion rate and any available data on the sensitizing heat treatment performed.

For example, many low-carbon and stabilized stainless steels e. Intergranular corrosion occurs as a result of precipitation of nitridescarbidesand other intermetallic phasessuch as sigma phase, that occurs along the grain boundaries.

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Choosing the correct method s rely on a complete understanding of your material and processes, as well as the concept of corrosion itself. Metals like stainless steels and aluminum contain elements such as niobium and chromium, often integrated because of their natural corrosion resistance.

Strauss test specimens are boiled in a Copper Sulfate – Sulfuric Acid mixture for 15 hours. Like what you saw? Intergranular corrosion practiec up as the dark black lines around the grain boundaries. Share on Tumblr Print. Our knowledgeable scientists have the experience and expertise necessary to determine the most appropriate intergranular attack testing methods for your material while providing actionable results you practixe rely on.

Because it can be run quickly for screening, we often run this test first. Methods for preparing the test specimens, rapid screening tests, apparatus setup and testing procedures, and calculations and practicee contents are described for each pracyice practice.

A bend test followed by a visual or micro-examination are used to determine “Pass” or “Fail” of test specimens. Classification of the structure after A Practice A analysis will determine if the material is acceptable or if additional testing is required.

Historical Version s – view previous versions of standard Work Item s – proposed revisions of this standard Translated Version s: The Strauss test is commonly used to evaluate the heat-treatment of as-received material, the effectiveness of alloying additions of elements such as Nb and Ti, or the effectiveness of reducing carbon content to resist intergranular attack.

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Sensitization causes the grain boundaries of a material to precipitate, creating carbide deposits and causing the material to be susceptible to intergranular attack. In many cases we can reduce that to as little as 24 hours more than the required testing time if you need fast results.

View more articles about Aerospace Oil and Gas Transportation. The etch structure types used to classify the specimens are: The Huey test works well to analyze chromium depleted regions and intermetallic precipitates, such as sigma phase, and is also used for materials in strongly oxidizing practcie such as nitric acid.

In everyday applications, corrosion varies by materials and solutions. However, when a f is exposed to high temperatures for long periods of time, a process called sensitization may occur. From macroscopic imaging to Scanning Electron Microscopy, Element provides turnkey metallographic services using state-of-the-art equipment. Historical Version s – view previous versions of standard. This specification covers the standard practices for detecting susceptibility to intergranular attack in austenitic stainless steels.

Corrosion Testing

How do you select the right ASTM corrosion testing method for practicce material? This test is used exclusively to determine corrosion in areas high in chromium carbide formations, and is not as effective for intergranular attack caused by other means. The weight loss is calculated after each step, and reveals if the sample has been properly heat-treated.

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